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The Silver Prospector | ||||||||
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10x – A Cadmium metal button, which is nearly as white as silver and Indium.
20x – A fragment of flattened Cadmium Metal being dissolved in 1 drop HNO3 and 2 drops H2O.When a little heat is applied to hasten the dissolving action of the HNO3 the rising vapors have the odor of coffee.
40x – A magnified view of a portion of the preceding image, attempting to focus upon the grain boundaries that resemble silver in similar circumstances.
25x – The preceding digestion is complete and a little heat applied to hasten the drying process, which produced this crystalline formation of Cadmium in a nitric acid solution. This dried supersaturated crystalline deposit may or may not be helpful in identifying Cd if other elements are present.
10x – 1 drop of water and 1 drop of HNO3 was applied to the preceding imaged dried solution and a single crystal of K2CrO7 (potassium dichromate) was inserted. The next 2 images show what happens when a little heat is applied to this solution.
10x – As heat was applied to the HNO3 solution the K2Cr2O7 crystal dissolved and these yellow crystals began growing.
25x – A magnified view of the preceding image to better illustrate the structure of the crystalline formations.
10x – A piece of Cd was dissolved in 1 drop HNO3 & 1 drop H2O. NOTE: Cd vigorously dissolves in concentrated HNO3 with the evolution of copious amounts of reddish nitrous oxide fumes.
10x – Because no precipitant formed and being impatient the glass slide was heated to initiate some sort of reaction, which this image indicates with this black deposition.
40x – This black precipitate resembled reduce Iodine crystals due to reacting with HNO3. However, upon further heating no reaction formed and these black crystals dissolved, which I have not seen occur before. Normally, too much heat will initiate a reaction between the Iodide and HNO3.
10x – This is the dried solution from preceding image containing HNO3, H2O, dissolved Cd and KI, which seemed to precipitate the black crystals that dissolved and formed this image of the dried solution. The next 6 images are solutions that concentrated HCl was utilized.
10x – A piece of Cadmium metal that was subject to 1 drop of HCl and gently heated to dry, which produced this white and tinge of blue super-saturated deposit rings. HCl does not dissolve Cadmium metal as easily nor as quickly as HNO3 does. In fact HCl is quite slow and needs a little heat to dissolve this metal.
10x – A single crystal of K2Cr2O7 was inserted in the HCl solution containing the amount of dissolved Cadmium in preceding image.
10x – The K2Cr2O7 crystal has dissolved, but no precipitant formed, so heat was applied to the glass slide, which formed this deposition when heat was applied to cause super-saturation.
30x – A magnified view of the lower right corner of the preceding image that better illustrates the near dry saturated crystalline structures that K2Cr2O7 helped create.
40x – A magnified view of the preceding image. I would not consider K2Cr2O7 as a reagent to determine the presence of Cadmium in a HCl solution. However, potassium dichromate would be beneficial to identify other metals in chemical combination with dissolved Cadmium.
10x – Another HCl solution that has digested another fragment of Cadmium metal.
10x – This toothpick tip was inserted in the acidic solution containing the dissolved Cadmium and ignited.
40x – This magnified view of the reignited preceding image and still no metal reduced.
40x – A magnified view of the preceding image, which was again ignited, but no metal was reduced.
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