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The purpose of this Iodine post is to illustrate some of the visual/chemical reactions of Potassium Iodine (KI) when mixed with various strengths of nitric acid.
10x – A solution of 1 drop nitric and 3 drops water produces no immediate reaction, but when another drop of nitric acid is added to this solution the previously dissolved KI produces an almost immediate (1 to 2 seconds) reaction as shown here.
10x – After about 10 seconds into the reaction the Iodine changed from the red-orange to brown and these zillions of the black crystals.
10x – Another test where the solution is composed of 1 drop nitric acid and 1 drop water and a single KI crystal inserted into the solution.
10x – The completed reaction of the above image.
10x – Another test, where the solution consisted of 1 drop of nitric and 1 drop of water.
10x – After about 10 seconds the previous image became this image.
50x – A magnified image of the preceding photomicrograph, which tries to focus in on the black Iodine crystals. Unfortunately they are ill defined at this magnification.
70x – Further magnification of the preceding image begins to show the crystal shape of the liberated/reduced Iodine. There are a metals that KI will precipitate as tiny black crystals from solutions of Nitric. Hydrochloric and Aqua-Regia. Click here to watch a few second, not entirely focused video of a reaction of KI crystals clinging to a toothpick tip being inserted into a solution of 1 drop nitric and 1 drop water on glass slide. The white background is to show as much color as practical. |
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